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The last phase of densi cation may involve temperatures considerably in excess of 100 C to complete the polymerization reaction and drive off the last amounts of solvent Fabrication of the silica gel, such as by coating onto some object or deice or pouring into a mold, can be carried out at various times during the overall process depending on the speci c application A variety of mixed silicate glasses can be obtained by including other compounds in the reaction mixture Borosilicate, aluminosilicate, and mixed boroaluminosilicate glasses containing various additional cations (eg, sodium, barium, potassium) are produced by polymerizing a mixture of tetraalkoxysilane with the appropriate alkoxides, acetates, or nitrates of the other metals Nonhydrolytic sol-gel synthesis is a more recent variation on the sol gel method A metal halide is reacted with an oxygen derivative of the metal (Eq 2-234).

The reaction is catalyzed by Lewis acids such as FeCl3 and alkyl halide is a by-product [Hay and Raval, 2001] The reaction has been used to produce alumina (Al2O3) and titania (TiO2) as well as silica [Corriu and Leclercq, 1996]..

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The crisis of high yields did not occur in Belgium in 1920, but, as in France, it occurred in 1925 1926 After 1926, Belgian yields fell to the American level or a little lower, whereas in France yields then fell far below the American level During the early 1930 s, Belgian yields tended to fluctuate with American yields, but after 1937 Belgian yields rose far above American yields In this they also followed the French pattern After 1946, the difference from other trends became very striking There was no great rise in the yield of the 4s from 1946 to 1960 such as there was in the yields of bonds in almost every other country studied American yields rose and met the yield of the Belgian 4s in 1959 While other Belgian issues yielded more than the 4s, the uptrend in yields in the 1950 s was unusually small..

2-234

Although inorganic polymers nd important applications as glasses and ceramics, their high rigidity make them unsuitable for replacement of organic polymers. Organometallic polymers, a compromise between inorganic and organic polymers, have been studied in the effort to achieve the goal of heat-resistant polymers processable by the techniques used for organic polymers. The general approach involves decreasing the extent of ladder, sheet, and threedimensional structures as well as bridging between different chains through cation oxygen anion interactions by replacing some of the oxygen linkages to metal atoms by organic linkages. The model for this approach is the polysiloxane system, where the presence of two organic groups attached to each silicon atom greatly changes chain rigidity compared to silica. Although many systems have and are being investigated, commercial success in this eld is limited at present. 2-15b-1 Polymerization via Reaction at Metal Bond

The first category, tone, is familiar to everyone already through the tone controls on your stereo. Bass and treble. But fuzz is also a tone variant, and similar distortions abound within bendable circuits. You ll also find interesting phasing and flanging effects added to the basic sounds of the circuit as you try different bends. Although some of these modulations can be very strange, we re still in familiar enough territory, and Jimi Hendrix s guitar in Purple Haze will still sound as though it s hitting the right notes no matter the tone. Essentially, when talking tone we re talking timbre, the reason a violin and circular saw sound different when playing the same note. It is the timbre, or wave-form, difference in these two voices that effects us emotionally one way or the other. So let the bent composer be able and the audience be warned!

Many polymerizations used to synthesize organometallic polymers involve cleavage of a bond to the metal atom of one reactant followed by attachment at that metal of a fragment derived from a second reactant [Carraher et al., 1978; Kaliyappan and Kannan, 2000; Manners, 1996; Nguyen et al., 1999; Pittman et al., 1987; Sheets et al., 1985]. A wide range of reactions have been used, but only a few are illustrated here. Carboxylate and sul de groups have been used to obtain organometallic polymers (Eqs. 2-235 and 2-236). These types of reactions have been used to synthesize organometallic polymers of a wide variety of other metals (e.g., Zr, Hf, Si, Ge, Pb, As, Sb, Bi, Mn, B, Se). The polymer obtained

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